小中大HPLC Troubleshooting——HPLC故障排除类文献综合 还是读硕士时整理的文献，自认为很有价值，来这里分享一下
HPLC Troubleshooting
Content
1. Scaling Gradient LC Methods to LC–MS
2. The Problem of Late Elution ---A Case Study
3. Reducing Column Diameter in Gradient Elution ---- A Case
Study
4. Unexpected Peaks
5. Autosampler Carryover
6. Reproducibility and Carryover ---- A Case Study
7. Buffers and Baselines
8. Communicating with the Baseline
9. When Ideal Isn’t Practical
10. Attacking Carryover Problems
11. Retaining Polar Compounds
12. Ion Suppression in LC-MS-MS ---- A Case Study
13. Quiet, Please
14. Stability-Indicating Assays
15. Peak Tailing and Resolution
16. The Importance of Temperature
17. Resolving Minor Peaks
18. Performance Qualification of LC Systems
19. The Hazards of Adjusting Gradients
20. Mobile-Phase Buffers, Part I ---- The Interpretation of pH in
Partially Aqueous Mobile Phases
21. Mobile-Phase Buffers, Part II ---- Buffer Selection and Capacity
22. Mobile-Phase Buffers, Part III ---- Preparation of Buffers
23. Success with Evaporative Light-Scattering Detection
24. LC Columns ---- The Top-10 List
25. Flow Rate and Peak Spacing
26. Not Another Leak!
27. Why Do Peaks Tail?
28. Extracolumn Effects
29. Broad Peaks
30. Understanding Split Peaks
31. Autosamplers ---- Symptoms and Solutions
32. Autosamplers, Part I ---- Design Features
33. Autosamplers, Part II ---- Problems and Solutions
34. The Cleaning and Regeneration of Reversed- Phase HPLC
Columns
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[ 本帖最后由 aasle 于 2010-8-6 11:43 编辑 ]
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