小中大【求助】向大家请教一个戴安ICS-5000的软件(变色龙6.80...
标签:pe mi ct 戴安 ta
色谱仪型号:戴安ICS-5000,自动进样器AS-DV
软件版本:变色龙6.80
程序设置的目的是:
第1个程序——只分析阴离子,与阴离子分析无关的部件处于关闭状态。
第2个程序——阴阳离子同时分析;
现在的问题是:阴阳离子同时分析是没有问题的。但是第1个程序,在实际操作中出现错误,无法运行。
下面把这两个程序都贴出来,希望有大虾指点一二。
阴离子进样
Column_TC.AcquireExclusiveAccess
Pump_2.Pressure.LowerLimit = 200 [psi]
Pump_2.Pressure.UpperLimit = 3000 [psi]
Pump_2.MaximumFlowRamp = 6.00 [ml/min2]
Pump_2.%A.Equate = "%A"
Pump_2.%B.Equate = "%B"
Pump_2.%C.Equate = "%C"
Pump_2.%D.Equate = "%D"
Pump_1.Pressure.LowerLimit = 200 [psi]
Pump_1.Pressure.UpperLimit = 3000 [psi]
Pump_1.MaximumFlowRamp = 6.00 [ml/min2]
Pump_1.%A.Equate = "%A"
Pump_1.%B.Equate = "%B"
Pump_1.%C.Equate = "%C"
Pump_1.%D.Equate = "%D"
EGC_1.CR_TC = Off
EGC_2.CR_TC = On
DeliverSpeed = 4.0 [ml/min]
DelayVolume = 125 [μl]
FlushFactor = 10
DeliverSample
Sampler.LoadPosition
DeliverSample Volume=Full
EndSamplePrep
CDet2.Data_Collection_Rate = 5.0 [Hz]
CDet2.Temperature_Compensation = 1.7 [%/°C]
Cell2Heater.Mode = On
Cell2Heater.TemperatureSet = 35.00 [°C]
Column_TC.Mode = On
Column_TC.TemperatureSet = 30.00 [°C]
Suppressor1.Type = CSRS_4mm
Suppressor1.CurrentSet = 80 [mA]
Suppressor1.Mode = off
Suppressor2.Type = ASRS_4mm
Suppressor2.CurrentSet = 100 [mA]
EGC_1.Concentration = 20.00 [mM]
EGC_1.Mode = Off
EGC_1.Curve = 5
EGC_2.Concentration = 30.00 [mM]
EGC_2.Curve = 5
Pump_1.Flow = 1.200 [ml/min]
Pump_1.Motor = Off
Pump_1.%B = 0.0 [%]
Pump_1.%C = 0.0 [%]
Pump_1.%D = 0.0 [%]
Pump_1.Curve = 5
Pump_2.Flow = 1.200 [ml/min]
Pump_2.%B = 0.0 [%]
Pump_2.%C = 0.0 [%]
Pump_2.%D = 0.0 [%]
Pump_2.Curve = 5
0.000 CDet2.Autozero
Wait CycleTimeState
Inject
CD_2.AcqOn
0.500 BeginOverlap
10.000 CD_2.AcqOff
Column_TC.ReleaseExclusiveAccess
End