小中大以后建议尽量传图片,方便他人尽快的回复。
lz的图片如下
相应的pdf卡片,六方,如下
PDF#15-0876: QM=Star(S); d=Diffractometer; I=(Unknown)
Fluorapatite, syn
Ca5 ( P O4 )3 F
Radiation=CuKa1 Lambda=1.54056 Filter=Ni
Calibration=Internal(W) 2T=10.887-63.298 I/Ic(RIR)=1.50
Ref: d:\应用软件\mdi jade 6.5 portable\pdf\codens.dat missing!
Hexagonal - Powder Diffraction, P63/m (176) Z=2 mp=
CELL: 9.3684 x 9.3684 x 6.8841 <90.0 x 90.0 x 120.0> P.S=hP42 (?)
Density(c)=3.201 Density(m)=3.150 Mwt=504.31 Vol=523.25 F(30)=73.7(.0120,34/0)
Ref: Ibid.
Strong Lines: 2.80/X 2.70/6 2.77/6 3.44/4 2.62/3 1.84/3 1.94/3 2.25/2 3.07/2 1.80/2
NOTE: Prepared at NBS, Gaithersburg, Maryland, USA, from Ca3 ( P O4 )2.
Spectroscopic analysis: 0.1 to 1.0% each of Mg and Na; and 0.01 to 0.1% each of Al, Ba, Ge, Fe, Si, and Sr.
Pattern taken at 25 C.
To replace 00-003-0736, 00-034-0011 and 00-035-0496.
See ICSD 1709 (PDF 01-070-0796); ICSD 1710 (PDF 01-070-0797); ICSD 9444 (PDF 01-071-0880); ICSD 9445 (PDF 01-071-0881); ICSD 24236 (PDF 01-073-1727); ICSD 27829; ICSD 27830; ICSD 30261 (PDF 01-075-0915); ICSD 34228 (PDF 01-076-0558); ICSD 66573 (PDF 01-079-1572); ICSD 75165 (PDF 01-082-1109); ICSD 79652 (PDF 01-083-0556); ICSD 79653 (PDF 01-083-0557).
2-Theta d(?) I(f) ( h k l) Theta 1/(2d) 2pi/d n^2
10.887 8.1200 8.0 ( 1 0 0) 5.443 0.0616 0.7738
16.874 5.2500 4.0 ( 1 0 1) 8.437 0.0952 1.1968
18.930 4.6840 <1 ( 1 1 0) 9.465 0.1067 1.3414
21.901 4.0550 8.0 ( 2 0 0) 10.950 0.1233 1.5495
22.949 3.8720 8.0 ( 1 1 1) 11.475 0.1291 1.6227
25.472 3.4940 <1 ( 2 0 1) 12.736 0.1431 1.7983
25.863 3.4420 40.0 ( 0 0 2) 12.932 0.1453 1.8254
28.153 3.1670 14.0 ( 1 0 2) 14.077 0.1579 1.9840
29.091 3.0670 18.0 ( 2 1 0) 14.546 0.1630 2.0486
31.936 2.8000 100.0 ( 2 1 1) 15.968 0.1786 2.2440
32.267 2.7720 55.0 ( 1 1 2) 16.134 0.1804 2.2667
33.127 2.7020 60.0 ( 3 0 0) 16.563 0.1850 2.3254
34.141 2.6240 30.0 ( 2 0 2) 17.071 0.1905 2.3945
35.640 2.5170 6.0 ( 3 0 1) 17.820 0.1986 2.4963
39.329 2.2890 8.0 ( 2 1 2) 19.665 0.2184 2.7449
40.040 2.2500 20.0 ( 3 1 0) 20.020 0.2222 2.7925
40.643 2.2180 4.0 ( 2 2 1) 20.321 0.2254 2.8328
42.193 2.1400 6.0 ( 3 1 1) 21.097 0.2336 2.9361
42.443 2.1280 4.0 ( 3 0 2) 21.221 0.2350 2.9526
43.893 2.0610 6.0 ( 1 1 3) 21.947 0.2426 3.0486
44.645 2.0280 2.0 ( 4 0 0) 22.323 0.2465 3.0982
45.377 1.9970 4.0 ( 2 0 3) 22.688 0.2504 3.1463
46.865 1.9370 25.0 ( 2 2 2) 23.432 0.2581 3.2438
48.266 1.8840 14.0 ( 3 1 2) 24.133 0.2654 3.3350
48.873 1.8620 4.0 ( 3 2 0) 24.436 0.2685 3.3744
49.583 1.8370 30.0 ( 2 1 3) 24.791 0.2722 3.4204
50.764 1.7970 16.0 ( 3 2 1) 25.382 0.2782 3.4965
51.563 1.7710 14.0 ( 4 1 0) 25.782 0.2823 3.5478
52.292 1.7480 14.0 ( 4 0 2) 26.146 0.2860 3.5945
53.143 1.7220 16.0 ( 0 0 4) 26.572 0.2904 3.6488
54.440 1.6840 <1 ( 1 0 4) 27.220 0.2969 3.7311
56.139 1.6370 6.0 ( 3 2 2) 28.070 0.3054 3.8382
57.283 1.6070 4.0 ( 3 1 3) 28.642 0.3111 3.9099
58.355 1.5800 2.0 ( 5 0 1) 29.178 0.3165 3.9767
59.094 1.5620 <1 ( 3 3 0) 29.547 0.3201 4.0225
60.283 1.5340 6.0 ( 4 2 0) 30.142 0.3259 4.0959
60.720 1.5240 4.0 ( 3 3 1) 30.360 0.3281 4.1228
61.751 1.5010 4.0 ( 2 1 4) 30.876 0.3331 4.1860
61.935 1.4970 4.0 ( 4 2 1) 30.967 0.3340 4.1972
63.298 1.4680 8.0 ( 5 0 2) 31.649 0.3406 4.2801